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Adsorption of fluoride on clay minerals and their mechanisms using X-ray photoelectron spectroscopy

Junyi DU, Daishe WU, Huayun XIAO, Ping LI

《环境科学与工程前沿（英文）》 2011年 第5卷 第2期   页码 212-226 doi: 10.1007/s11783-010-0255-5

摘要： This research investigates the adsorption mechanisms of fluoride (F) on four clay minerals (kaolinite, montmorillonite, chlorite, and illite) under different F concentrations and reaction times by probing their fluoride superficial layer binding energies and element compositions using X-ray photoelectron spectroscopy (XPS). At high F concentrations ( = 5–1000 mg·L ), the amount of F adsorbed ( ), amount of hydroxide released by clay minerals, solution F concentration, and the pH increase with increasing . The increases are remarkable at >50 mg·L . The increases significantly by continuously modifying the pH level. At <5–100 mg·L , clay minerals adsorb H to protonate aluminum-bound surface-active hydroxyl sites in the superficial layers and induce F binding. As the increases, F , along with other cations, is adsorbed to form a quasi-cryolite structure. At >100 mg·L , new minerals precipitate and the product depends on the critical Al concentration. At [Al ]>10 mol·L , cryolite forms, while at [Al ]<10 mol·L , AlF is formed. At low (0.3–1.5 mg·L ), proton transfer occurs, and the F adsorption capabilities of the clay minerals increase with time.

关键词： clay mineral     fluoride (F)     adsorption mechanism     X-ray photoelectron spectroscopy (XPS)    

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建材非金属矿产资源强国战略研究

顾真安,同继锋,崔源声,彭寿,苏桂军,周洪锦,冯惠敏,赵飞,田桂萍,孟庆洁,洪伟

《中国工程科学》 2019年 第21卷 第1期   页码 104-112 doi: 10.15302/J-SSCAE-2019.01.015

摘要：

本文研究我国主要建材产品生产所用的水泥灰岩、玻璃用硅质原料、建筑卫生陶瓷用黏土矿原料（高岭土）、高纯石英和石墨五种非金属矿产资源的强国建设战略，确定建材非金属矿产资源发展的战略思路与目标，指出加强矿区规划与保护、建设供应示范基地和标准原料基地、加快推进战略性资源储备制度等重点任务，提出设立矿产资源强国建设领导小组、完善矿产资源原料产品标准体系建设、加强人才培养体系建设、加强矿产资源法律法规制定与实施等保障措施。

关键词： 建材     强国战略     水泥灰岩     玻璃用硅质原料     建筑卫生陶瓷用黏土矿原料（高岭土）     高纯石英     石墨    

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Bearing and uplift capacities of under-reamed piles in soft clay underlaid by stiff clay using lower-bound

Mantu MAJUMDER, Debarghya CHAKRABORTY

《结构与土木工程前沿（英文）》 2021年 第15卷 第2期   页码 537-551 doi: 10.1007/s11709-021-0708-x

摘要： Ensuring a safe foundation design in soft clay is always a challenging task to engineers. In the present study, the effectiveness of under-reamed piles in soft clay underlaid by stiff clay is numerically studied using the lower-bound finite element limit analysis (LB FELA). The bearing and uplift capacities of under-reamed piles are estimated through non-dimensional factors and , respectively. These factors increased remarkably and marginally compared to and of the piles without bulbs when the bulb is placed in stiff and soft clay, respectively. For a given ratio of undrained cohesion of stiff to soft clay ( / ), the factors and moderately increased with the increase in the length-to-shaft-diameter ratio ( / ) and adhesion factors in soft clay ( ) and stiff clay ( ). The variation of radial stress along the pile–soil interface, distribution of axial force in the under-reamed piles, and state of plastic shear failure in the soil are also studied under axial compression and tension. The results of this study are expected to be useful for the estimation of the bearing and uplift capacities of under-reamed piles in uniform clay and soft clay underlaid by stiff clay.

关键词： bearing capacity     uplift capacity     under-reamed pile     clay     limit analysis    

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Model testing of tripod caisson foundations in silty clay subjected to eccentric lateral loads

《结构与土木工程前沿（英文）》 2023年 第17卷 第3期   页码 467-476 doi: 10.1007/s11709-023-0933-6

摘要： In this study, model tests were conducted to investigate the bearing capacities of tripod caisson foundations subjected to eccentric lateral loads in silty clay. Lateral load–rotation curves of five eccentric-shaped tripod suction foundations were plotted to analyze the bearing capacities at different loading angles. It was observed that the loading angle significantly influenced the bearing capacity of the foundations, particularly for eccentric tripod caisson foundations. Compared with eccentric tripod caisson foundations, the traditional tripod foundation has a relatively high ultimate lateral capacity at the omnidirectional loading angle. By analyzing the displacement of the caissons, a formula for the rotational center of the tripod caisson foundation subjected to an eccentric lateral load was derived. The depth of the rotation center was 0.68–0.92 times the height of the caisson when the bearing capacity reached the limit. Under the undrained condition, suction was generated under the lid of the “up-lift” caisson, which helps resist lateral forces from the wind and waves.

关键词： tripod caisson foundation     silty clay     eccentric lateral capacity     model tests    

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Behavior of compacted clay-concrete interface

R. R .SHAKIR, Jungao ZHU

《结构与土木工程前沿（英文）》 2009年 第3卷 第1期   页码 85-92 doi: 10.1007/s11709-009-0013-6

摘要： Tests of interface between compacted clay and concrete were conducted systematically using interface simple shear test apparatus. The samples, having same dry density with different water content ratio, were prepared. Two types of concrete with different surface roughness, i.e., relatively smooth and relatively rough surface roughness, were also prepared. The main objectives of this paper are to show the effect of water content, normal stress and rough surface on the shear stress-shear displacement relationship of clay-concrete interface. The following were concluded in this study: 1) the interface shear sliding dominates the interface shear displacement behavior for both cases of relatively rough and smooth concrete surface except when the clay water content is greater than 16% for the case of rough concrete surface where the shear failure occurs in the body of the clay sample; 2) the results of interface shear strength obtained by direct shear test were different from that of simple shear test for the case of rough concrete surface; 3) two types of interface failure mechanism may change each other with different water content ratio; 4) the interface shear strength increases with increasing water content ratio especially for the case of clay-rough concrete surface interface.

关键词： soil structure interaction     simple shear test     interface     friction     compacted clay     interface modeling    

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Analysis of cement-treated clay behavior by micromechanical approach

Dong-Mei ZHANG, Zhen-Yu YIN, Pierre-Yves HICHER, Hong-Wei HUANG

《结构与土木工程前沿（英文）》 2013年 第7卷 第2期   页码 137-153 doi: 10.1007/s11709-013-0204-z

摘要： Experimental results show the significant influence of cement content on the mechanical properties of cement-treated clays. Cementation is produced by mixing a certain amount of cement with the saturated clay. The purpose of this paper is to model the cementation effect on the mechanical behavior of cement-treated clay. A micromechanical stress-strain model is developed considering explicitly the cementation at inter-cluster contacts. The inter-cluster bonding and debonding during mechanical loading are introduced in two ways: an additional cohesion in the shear sliding and a higher yield stress in normal compression. The model is used to simulate isotropic compression and undrained triaxial tests under various confining stresses on cement-treated Ariake clay and Singapore clay with various cement contents. The applicability of the present model is evaluated through comparisons between numerical and experimental results. The evolution of local stresses and local strains in inter-cluster planes are discussed in order to explain the induced anisotropy due to debonding at contact level under the applied loads. The numerical simulations demonstrate that the proposed micromechanical approach is well adapted for taking into account the main physical properties of cement-treated clay, including damage and induced anisotropy under mechanical loading.

关键词： microstructure     cementation     clay     micromechanics     anisotropy     debonding    

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Experimental investigation of the influence on static and cyclic deformation of structural soft clay

CHEN Yunmin, CHEN Yingping, HUANG Bo

《结构与土木工程前沿（英文）》 2007年 第1卷 第4期   页码 422-429 doi: 10.1007/s11709-007-0057-4

摘要： This paper presents the experimental results performed to study the static and cyclic deformation behavior of undisturbed and remolded soft clays sampling from Xiaoshan. The consolidation tests indicated that the vertical strains of

关键词： consolidation     deformation     experimental     undisturbed    

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Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd KIEVANI, Milad EDRAKI

《化学科学与工程前沿（英文）》 2015年 第9卷 第1期   页码 40-45 doi: 10.1007/s11705-015-1505-7

摘要： Nano-clay based pigments (NCP) are new type of pigments composed of organic dyes and layered silicate-clay nano-particles, and have already been used in polymeric coatings to improve mechanical thermal and stability properties. In this paper, the basic blue 41(BB41) was intercalated into Na - montmorillonite in an aqueous medium. The dye-intercalated montmorillonite was centrifuged, dried, and milled to prepare the nanopigment particles. X-ray diffraction showed an increase in the basal spacing, thus confirming intercalation of the BB41 molecules within the nanostructures of the interlayer spaces. Fourier transform infrared spectroscopy was used for identifying the functional groups and chemical bounding of Na -montmorillonite, BB41 and montmorillonite-BB41. The morphology of NCP was also studied by transmission electron microscopy. Finally, thermo-gravimetric analysis and differential thermograms suggested the thermal stability of the intercalated dye was improved.

关键词： nanopigment     layered silicate     cationic dye     thermal properties    

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Ultimate bearing capacity of strip footing resting on clay soil mixed with tire-derived aggregates

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 1016-1024 doi: 10.1007/s11709-021-0751-7

摘要： This study investigated the use of recycled tire-derived aggregate (TDA) mixed with kaolin as a method of increasing the ultimate bearing capacity ( UBC) of a strip footing. Thirteen 1g physical modeling tests were prepared in a rigid box of 0.6 m × 0.9 m in plan and 0.6 m in height. During sample preparation, 0%, 20%, 40%, or 60% (by weight) of powdery, shredded, small-sized granular (G 1–4 mm) or large-sized granular (G 5–8 mm) TDA was mixed with the kaolin. A strip footing was then placed on the stabilized kaolin and was caused to fail under stress-controlled conditions to determine the UBC. A rigorous 3D finite element analysis was developed in Optum G-3 to determine the UBC values based on the experimental test results. The experimental results showed that, except for the 20% powdery TDA, the TDA showed an increase in the UBC of the strip footing. When kaolin mixed with 20% G (5–8 mm), the UBC showed a threefold increase over that for the unreinforced case. The test with 20% G (1–4 mm) recorded the highest subgrade modulus. It was observed that the UBC calculated using finite element modeling overestimated the experimental UBC by an average of 9%.

关键词： kaolin     physical modeling tests     stabilization     numerical modeling    

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Optimized porous clay heterostructure for removal of acetaldehyde and toluene from indoor air

Pu ZHAO,Lizhong ZHU

《环境科学与工程前沿（英文）》 2016年 第10卷 第2期   页码 219-228 doi: 10.1007/s11783-014-0760-z

摘要： Adsorption is the most widely used technology for the removal of indoor volatile organic compounds (VOCs). However, existing adsorbent-based technologies are inadequate to meet the regulatory requirement, due to their limited adsorption capacity and efficiency, especially under high relative humidity (RH) conditions. In this study, a series of new porous clay heterostructure (PCH) adsorbents with various ratios of micropores to mesopores were synthesized, characterized and tested for the adsorption of acetaldehyde and toluene. Two of them, PCH25 and PCH50, exhibited markedly improved adsorption capability, especially for hydrophilic acetaldehyde. The improved adsorption was attributed to their large micropore areas and high micropore-to-mesopore volume ratios. The amount of acetaldehyde adsorbed onto PCH25 at equilibrium reached 62.7 mg·g , eight times as much as the amount adsorbed onto conventional activated carbon (AC). Even at a high RH of 80%, PCH25 removed seven and four times more of the acetaldehyde than AC and the unmodified raw PCHs did, respectively. This new PCH optimized for their high adsorption and resistance to humidity has promising applications as a cost-effective adsorbent for indoor air purification.

关键词： porous clay heterostructure     volatile organic compounds     adsorption     adsorbent     indoor air    

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Effects of exercise therapy on bone mineral density in early postmenopausal women: a controlled trial

Shilin DENG MD ,

《医学前沿（英文）》 2009年 第3卷 第3期   页码 323-329 doi: 10.1007/s11684-009-0061-2

摘要： The purpose of this article is to determine the effect of a well-designed combined aerobic, resistance, and extension exercise program on bone mineral density (BMD) in postmenopausal women. The population comprised 45 postmenopausal women, who exercised over 12months (exercise group), and 36 women who served as a non-training control group. BMD of the hip, and lumbar spine was measured at the baseline and 12th month. Repeated measurement analysis of variance and nonparametric test were utilized to compare differences between the exercise group and controls. Thirty-six out of 45 persons in the exercise group and 36 controls completed the study. Average compliance was 82.2% for the whole exercise group at the 12th month. All the subjects had decreased BMD, but the rate of bone loss was lower in the exercise group than in the control group at the L4 and hip. Although the exercise program in this study may probably reduce the rate of bone loss in weight-bearing skeletal sites, we do not suggest the exercise by itself be viewed as prevention or treatment for osteoporosis. Further, the exact dose-response relationship of exercise and bone mass in early postmenopause is not clear.

关键词： early postmenopausal women     bone mineral density     exercise     effects    

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矿物浮选吸附平衡模型构建与应用：精准解析矿物 表面离子 / 药剂特征吸附

高雅,付心壮,韩海生,王丽,岳彤,孙伟

《中国工程科学》 2023年 第25卷 第6期   页码 248-258 doi: 10.15302/J-SSCAE-2023.07.020

摘要：

矿物浮选吸附平衡模型是准确描述矿物浮选过程中所涉及的矿物表面离子 / 药剂吸附平衡的数学模型，首次实现了矿物表面位点与浮选药剂吸附作用亲和性的量化解析。传统浮选理论对矿物表面作用位点缺乏科学描述，难以阐明浮选药剂的吸附作用能力及平衡状态，新浮选药剂体系开发多以“试错法”“复配法”等经验性方法为主。药剂选择性吸附作为浮选作业的核心机制，若不能准确预测其在各矿物表面的吸附行为，将严重限制浮选工艺智能化控制的发展。本文详细论述了矿物浮选吸附平衡模型的构建原理，以赤铁矿 ‒ 石英和一水硬铝石 ‒ 高岭石两个浮选体系为例，通过对少量实验数据的拟合计算，解析出矿物表面活性位点密度Ns、加 / 去质子反应常数Kt1/Kt2、药剂吸附常数Kf等矿物浮选特征常数。将解析的矿物浮选特征常数代入到平衡模型中，预测出各条件下矿物表面电性、离子及浮选药剂的吸附量，通过零电点、实验及测试等方法验证了可靠性，形成了矿物浮选过程预测系统的内核算法。该算法对各条件下每种矿物药剂吸附的初步准确预测，可在一定程度上反映其可浮性趋势，有助于缩短浮选工艺开发周期，对矿物表面药剂吸附机理研究、浮选药剂分子设计、浮选工艺流程优化及智能控制等具有重要意义。

关键词： 矿物加工；浮选机理；矿物浮选吸附平衡模型；可浮性预测；矿物浮选特征常数    

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Relationship between the development of energy and mineral resources and ecological conservation redline

Dawei ZHANG

《工程管理前沿（英文）》 2019年 第6卷 第4期   页码 557-563 doi: 10.1007/s42524-019-0077-5

摘要： From a philosophical point of view, this study discusses the dialectical relationship between the development of energy and mineral resources and the ecological conservation redline. We propose that the ecological conservation redline and the development of energy and mineral resources should be guided by ecological civilization construction, that is, the energy and mineral resources should be rationally developed under the condition that the ecological environment is protected. This study analyzes the influence of the development of energy and mineral resources on the ecological environment. The handling of mining rights within the ecological conservation redline based on the law and the reduction of the influence of the development of energy mineral resources on the ecological environment by science and technology are presented. The environmental assessment system and technical standards for energy and mineral development are suggested to implement policies and measures for the disposal of mining rights within the redline and facilitate technological innovations of ecological conservation for energy and mineral development. Hence, a coordinated development between the ecological conservation redline and the development of energy and mineral resources can be promoted.

关键词： ecological conservation redline     development of energy and mineral resources     coordinated development    

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A state-of-the-art review on interfacial behavior between asphalt binder and mineral aggregate

Meng GUO, Yiqiu TAN, Linbing WANG, Yue HOU

《结构与土木工程前沿（英文）》 2018年 第12卷 第2期   页码 248-259 doi: 10.1007/s11709-017-0422-x

摘要： The interface between asphalt binder and mineral aggregate directly affects the service life of pavement because the defects and stress concentration occur more easily there. The interaction between asphalt binder and mineral aggregate is the main cause of forming the interface. This paper presents an extensive review on the test technologies and analysis methods of interfacial interaction, including molecular dynamics simulation, phase field approach, absorption tests, rheological methods and macro mechanical tests. All of the studies conducted on this topic clearly indicated that the interfacial interaction between asphalt binder and mineral aggregate is a physical-chemical process, and can be qualitatively characterized by microscopical technique (such as SEM and AFM), and also can be quantitatively evaluated by rheological methods and interfacial mechanical tests. Molecular dynamics simulation and phase field approach were also demonstrated to be effective methods to study the interfacial behavior and its mechanism.

关键词： Asphalt binder     Mineral aggregate     Interfacial behavior     Multiscale    

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Retraction note to: Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd Kievani,Milad Edraki

《化学科学与工程前沿（英文）》 2016年 第10卷 第3期   页码 440-440 doi: 10.1007/s11705-016-1573-3

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标题 作者 时间 类型 操作

Adsorption of fluoride on clay minerals and their mechanisms using X-ray photoelectron spectroscopy

Junyi DU, Daishe WU, Huayun XIAO, Ping LI

期刊论文

建材非金属矿产资源强国战略研究

顾真安,同继锋,崔源声,彭寿,苏桂军,周洪锦,冯惠敏,赵飞,田桂萍,孟庆洁,洪伟

期刊论文

Bearing and uplift capacities of under-reamed piles in soft clay underlaid by stiff clay using lower-bound

Mantu MAJUMDER, Debarghya CHAKRABORTY

期刊论文

Model testing of tripod caisson foundations in silty clay subjected to eccentric lateral loads

期刊论文

Behavior of compacted clay-concrete interface

R. R .SHAKIR, Jungao ZHU

期刊论文

Analysis of cement-treated clay behavior by micromechanical approach

Dong-Mei ZHANG, Zhen-Yu YIN, Pierre-Yves HICHER, Hong-Wei HUANG

期刊论文

Experimental investigation of the influence on static and cyclic deformation of structural soft clay

CHEN Yunmin, CHEN Yingping, HUANG Bo

期刊论文

Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd KIEVANI, Milad EDRAKI

期刊论文

Ultimate bearing capacity of strip footing resting on clay soil mixed with tire-derived aggregates

期刊论文

Optimized porous clay heterostructure for removal of acetaldehyde and toluene from indoor air

Pu ZHAO,Lizhong ZHU

期刊论文

Effects of exercise therapy on bone mineral density in early postmenopausal women: a controlled trial

Shilin DENG MD ,

期刊论文

矿物浮选吸附平衡模型构建与应用：精准解析矿物 表面离子 / 药剂特征吸附

高雅,付心壮,韩海生,王丽,岳彤,孙伟

期刊论文

Relationship between the development of energy and mineral resources and ecological conservation redline

Dawei ZHANG

期刊论文

A state-of-the-art review on interfacial behavior between asphalt binder and mineral aggregate

Meng GUO, Yiqiu TAN, Linbing WANG, Yue HOU

期刊论文

Retraction note to: Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd Kievani,Milad Edraki

期刊论文